SCI論文中怎樣描述TEM結果？

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前言:

鑒於有同學問我對於SCI論文寫作這個部分的更新計劃，我在這裡稍微跟大家說一下。這個部分肯定不僅僅是列出一些常規實驗結果如何描述這麼簡單。現在發的這些呢，只是一些基礎準備。在將這些準備工作做完了之後，我們會按照論文的結構，對每個部分進行詳細討論，儘可能把我們這些年學到的有用的東西分享給大家，給大家提供一些參考，幫助大家更快更好地掌握這個部分。還是那句話，科研辛苦，大家一起走才會走得更長久。希望能夠真正地幫助到各位，如果大家有更好地方式，願意分享的話，請隨時聯繫我們，謝謝！

1. 詳細描述樣品有著怎樣的形貌，由哪些微觀結構組成

實例一：Figure 1a shows a typical low-magnification transmission electron microscopy (TEM) image of the synthesized Co3O4, in which a batch of nanorods is developed from a cluster core, forming a coral-like morphology. Most of the nanorods have straight sides and regular ends, as shown in Fig. 1b, an enlarged TEM image.

(Ref.: Xie,X. et al. Nature, 2009,458, 746-749)

句式模板：Figure _ shows a typical low-magnification transmission electron microscopy (TEM) image of the synthesized __, in which a batch of __ is developed from __, forming __ morphology. Most of the __ have __, as shown in Fig. _, an enlarged TEM image.

實例二: Atomic-resolution HAADF images of the gold particles inthis sample reveal that they display a mixture of cub-octahedral (Fig.2a), singly twinned (Fig. 2b) and multiply twinned (Fig. 2c) morphologies, with the twinned variants dominating.

(Ref.: Lopez-Sanchez,J. et al. Nat. Chem. 2011, 3, 551-556)

句式模板：Atomic-resolution HAADF images of __ in this sample reveal that they display a mixture of __, __ and __ morphologies, with the __ dominating.

實例三：Transmission electron microscopy (TEM) studies reveal that the calcined BS-mTiO2possesses a two-dimensional hexagonal mesophase.

(Ref.: Liu, X. et al. Chem. Commun. 2010, 46, 6729-6731)

句式模板：Transmission electron microscopy (TEM) studies reveal that __ possesses a __ mesophase.

變型1：The material has a __ mesostructure as determined by transmission electron microscopy (TEM).

變型2：A typical TEM image, as presented in Figure _, indicates an __ with a diameter of about _ nm.

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2. TEM結果描述樣品的尺寸分布情況

實例一：A particle count taken from many such images, obtained from different regions of the sample,confirmed the presence of essentially monodispersed Au particles of mean diameter 1.4 nm, which is the expected size of Au55.

(Ref.: Turner, M. et al. Nature 2008, 454, 981-983)

句式模板：A particle count taken from many such images, obtained from different regions of the sample, confirmed the presence of essentially monodispersed __ particles of mean diameter _ nm, which is the expected size of __.

實例二：Transmission electron microscopy (TEM) analysis found that the metal NPs in the Pt/SiO2 (Fig. 3A) and Pt-Fe/SiO2(Fig. 3B) samples are anchored evenly over the silica hosts and have a narrow distribution in average size of 2 to 3 nm and 2 to 4 nm, respectively.

(Ref.: Fu,Q. et al. Science, 2010, 328, 1141-1144)

句式模板：Transmission electron microscopy (TEM) analysis found that the metal NPs in the __ samples are anchored evenly over the __ hosts and have a narrow distribution in average size of _ to _ nm and _ to_ nm, respectively.

實例三：As can be seen from Fig. 1a, the PtPdNPs are well dispersed in the m-SiO2 framework and the sizes of PtPd alloy NPs are rather small with a narrow size distribution(4.1 ± 0.6 nm).

(Ref.: Liu,J. et al. Catal. Sci. Technol. 2014, 4, 441–446)

句式模板：As can be seen from Fig. _, the __ NPsare well dispersed in the __ framework and the sizes of __ NPs are rather small with a narrow size distribution (_ ± _ nm).

變型：In more detail, the enlarged TEM image in Fig. __ shows that the __ nanoparticlesare _ nm in size and densely and uniformly distributed in amorphous mesoporous__. (Ref.: Qiu, Y. et al. Chem. Commun.2010, 46,8359-8361)

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3. HRTEM結果描述樣品的晶格條紋等微觀結構信息

實例一：High-resolution transmission electron microscopy (HRTEM) was used to characterize the catalysts after reaction (Figure 4). The Au-0.0 sample shows the characteristic spacings of 0.144 and0.235 nm for the (220) and the(111) lattice planes of FCC metallic gold.The AuCN-1.0 sample(right panels) shows the expected spacings of 0.306 and 0.312 nm for the (012) and (101) lattice planes ofNa[Au(CN)2].

(Ref.: Oyama, S. et al. ChemCatChem 2010, 2, 1582-1586)

句式模板：High-resolution transmission electronmicroscopy (HRTEM) was used to characterize the catalysts after reaction. The__ sample shows the characteristic spacings of _ and _ nm for the __ and the __lattice planes of FCC __. The __ sample shows the expected spacings of _ and _nm for the_and _lattice planes of __.

實例二：High-resolution TEM (HRTEM) images (Fig. 3, A and B, insets) show that NPs over both Pt/SiO2and Pt-Fe/SiO2 samples present the same face-centeredcubic ( FCC) Pt lattice with a Pt(111) interlayer spacing of 0.23 nm.

(Ref. : Fu, Q. et al. Science, 2010, 328, 1141-1144)

句式模板：High-resolution TEM (HRTEM) images show that NPs over __ samples present the same __ lattice with a __ interlayerspacing of _ nm.

實例三：As shown in Fig. 1c, the lattice fringes of Pt1Pd3 display interplanar spacings of 0.223 and 0.192nm in the particle, which match well respectively with those of the (111) and the (200) planesof the fccPtPd alloy.

(Ref.: Liu, J. et al. Catal. Sci.Technol. 2014, 4, 441–446)

句式模板：As shown in __, the lattice fringes of__ display interplanar spacings of _ and _ nm in the particle, which match well respectively with those of the __ and the __ planes of the fcc __.

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